Neuer Weg zur Synthese von chiralen 1,2,4-Oxadiazin-5-onen: einfache Synthese von neuen chiralen 1,2,4-Oxadiazin-5-onen aus natürlichen Aminosäuren
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Diese werden anschließend mit Thionylchlorid gefolgt von Methanol zu den entsprechenden α-Bromoestern reagieren. Die Kondensation dieser zuvor hergestellten α-Bromester mit 1-Benzen-sulfonylpyrrolidin-2-carboxamidoxim in Gegenwart von zwei Äquivalenten Natriumhydrid liefert die gewünschten neuen chiralen 1,2,4-Oxadiazin-5-one mit guten chemischen Ausbeuten.
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