Extração e estrutura cristalina da fisalina B
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4996(2), b = 14. 35620(10), c = 14.
75190(10)Å, V = 2607. 97(5)Å3, Z = 4,Dc = 1.
382mg/cm3, Mr = 542. 56, F(000) = 1152, e μ= 0.
870 mm-1. O R final = 0,0389 e wR = 0,1037 para 47670 reflexões observadas (I > 2ο(I)).
A molécula rígida é constituída por oito anéis fundidos envolvendo duas lactonas. Existem duas moléculas de C28H32O9 numa unidade simétrica, e o composto do título é empilhado numa estrutura de camada 3D através de ligações de hidrogénio.
Na gama de 5-20μmol/L, a fisalina B pode inibir significativamente a secreção de citocinas inflamatórias TNF-α e IL-6 em células RAW264. 7.
Os resultados sugerem que a fisalina B tem atividade anti-inflamatória in vitro. .
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